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Both methods effectively removed signal shift after being applied on measurement data acquired with five commercial instruments of identical configuration with quartz micro balance (QMB) sensor arrays.
The sample is brought to rest at the bottom of the chute and dislodged powder is collected in a micro balance incorporated inside a Faraday cage.
We have also used an ultra micro balance to determine the mass and mean single-layer surface coverage of each multilayer.
The instrument design combines three types of sensors to monitor in situ the dust mass flux (micro balance system, MBS) and single grain properties (grain detection system, GDS + impact sensor, IS).
In contrast, 'acoustic' mass, calculated from quartz crystal micro balance with dissipation monitoring, showed the lowest mass and dissipation values for CS2.6 (highest sulfation degree) multilayers indicating formation of stiffer layers compared to heparin and CS1.6 layers which led to higher mass and dissipation values.
An over-stoichiometric amount of deposited Au hinted at by the electrochemical quartz-crystal micro balance (EQCM) kinetic experiments and validated by separate pulse experiments has been attributed to reduction in each SLRR event of a pre-adsorbed layer of [AuCl4]− ions.
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The kinetics of tarnishing was tracked by reflectance, quartz-micro balance measurements, and electrochemical impedance spectroscopy.
The filters were placed in desiccators for ∼24 hrs before and after the sampling to remove the absorbed water and weighed in a controlled environment chamber after taking the filters out of the desiccators before and after the sampling using a semi-micro balance (Sartorius, Model ME 235 P).
The dry weight and dimensions of each membrane were then recorded using a micro-balance and micrometer.
The growth of the film thickness was monitored in-situ during the evaporation by a water cooled quartz micro-balance.
Experience on micro-balance performance study by dust deposition has been acquired and water vapour deposition studies are in progress in a Martian atmosphere simulation chamber.
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