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Sep-Pak tC18 Plus Short cartridges (400 mg) were obtained from Waters (Milford, MA).
Compound 13 (2.5 mg) were obtained from Fr-1 by HPLC eluting with 20%CH3CN/H2OO.
The highest values of soil pH, Ca and Mg were obtained under wood ash application, while the highest values of soil O.M and moderate values of soil P, K, Ca and Mg were obtained under poultry manure application.
Purified saccharides 1 (2.5 mg), 2 (2.2 mg) and 3 (2.0 mg) were obtained as white powders.
Working electrodes in the form of 1 cm diameter pellets (ca. 15 mg) were obtained by pressing the mixture.
Compounds 16 (6 mg), 17 (11 mg), and 18 (15 mg) were obtained from Frs. 2 by repeated prep.
Similar(16)
A yellowish powdered compound 1 (21 mg) was obtained.
From fraction 8, after preparative TLC, 4 (5 mg) was obtained.
The organic extract was evaporated to dryness and a dark oily residue (85 mg) was obtained.
After evaporation of the solvent, a dark oily residue (84 mg) was obtained.
Compound 6 (162 mg) was obtained from F2 by MCI CC (MeOH/H2O, 5→25 %).
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