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In the laser flash technique, disc shaped samples were prepared, either by hot pressing approximately 50 mg of material, or by cutting the discs from long cylindrical bars.
In this work we report on the protocol which standardizes measurements in TEM, SEM, TGA, Raman and UV VIS spectrometer, consumes <30 mg of material, and was found to provide fast and reliable feedback in the development of purification techniques.
Figure 2c was measured from sample E which contained about 3.6 mg of material and with NiO weight ratio of 38%.
To fabricate GCEs, 5 mg of material was mixed with 50 μL Nafion ethanol solution (5%) and 450 μL DI water.
Figure 2a was measured from sample B which originally contained about 4.2 mg of material and with a NiO weight ratio of 20%.
4 7 mg of material was heated in an alumina crucible under a 30 ml min−1 flow of air from 50 to 950 °C at a ramp rate of 10 °C min−1.
Similar(41)
A similar effectively instantaneous adsorption of ca. 1 mg m 2 of material at hydrophobic silica was observed for all formulations; an example is seen in Figure 5.
Photoreaction was conducted in a batch reactor (100 250 mL) containing 10 25 mg of materials under stirring conditions with a UV lamp flux of about 1 mW cm−2.
A 1 mg sample of material was removed from the resinous portion of each artefact.
Total organic carbon (TOC) was determined by direct combustion of 10 mg aliquots of material in a combustion furnace at 680 °C using an Apollo 9000 Total Organic Carbon Analyser fitted with a boat sampler (Model 183 Teledyne Tekmar, Mason, OH).
Samples were collected in three biological replicates per genotype and each sample (65 250 mg) consisted of material pooled from six plants.
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