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NiL2(Ph)2·xH2O [L=3,5-dimethylpyrazole or N-methyl imidazole; Ph=DCP or TCP; x=0, 1 or 3] complexes were synthesised and characterised by analytical and spectroscopic methods using elemental analysis and FTIR.
Methods using elemental loaded labels for enhancement of sensitivity and robustness of biomolecules quantification are gaining prominence and a number of key papers have been published [8,18,21,33,76 81].
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Obsidian is widely considered an ideal material for source tracing using elemental methods of analysis.
The macrobicyclic complexes synthesized were characterized using elemental analysis, spectroscopic methods, X-ray crystallography and cyclic voltammetry.
Two new coordination solids, [Cu2(µ tp)(phen 4](NO3 2.2H2O (1) and [Cu(pa 2 NO3)(H2O)]NO3.H2O (2) (phen = 1,10-phenanthroline, tp = terephthalate, pa = picolinamide), were synthesized from purely aqueous media and characterized using elemental analysis, spectroscopic methods (IR, UV vis NIR and ESR) and the single crystal X-ray diffraction technique.
The compositions of the solid acids were characterized using elemental analysis and thermogravimetric analysis methods.
A series of six novel benzimidazole-pyrazole hybrid molecules was synthesized and characterized using elemental analysis (CHN) and spectroscopic methods (1HNMR, FT-IR).
The compounds (1) and (2) were characterized using elemental analyses, spectral and other physicochemical methods.
Microanalysis was conducted using elemental analyzer 106.
The methods used for elemental and bulk isotopic analyses are described by Takano et al. (2012).
Recently, Ward et al. have described methods using a soft clustering approach employing multiple Gaussian fits to elemental correlation plots, and assignment of pixel-probability to groups (each represented by a Gaussian) to effectively relax group membership criteria.
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