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The subsequent methods for fatty acid methyl ester (FAME) preparation and gas chromatographic (GC) analysis are the same as reported by Wang [ 32].
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A new analytical method for fatty acid alkyl esters (FAAEs) determination by GC MS in virgin olive oils is proposed.
A rapid method for fatty acids (FAs) comparative profiling based on carboxyl-specific stable isotope labeling (SIL) and direct infusion electrospray ionization ion mobility mass spectrometry (ESI IM MS) is established.
14 Computed tomography (CT) scan is a widely used, less invasive method for fatty liver disease detection.
Liver biopsy is probably the most reliable method for fatty liver diagnosis, but this procedure is associated with some morbidity and mortality.
This study is the first report of an automated method for fatty-acid analysis of the phospholipid fraction of human plasma, which includes both phospholipid extraction and FAME derivatization, and has been successfully applied to date to more than 28,000 samples of the InterAct project (detailed information about the subjects can be found in the cohort description [ 17]).
Aim of this study was to compare three methods for determining fatty acid (FA) profiles in ruminant feces by GC.
A few validation analyses were performed to ensure the reliability of the method used for fatty acid analysis in this study; these measures included linearity, precision (repeatability and reproducibility), and recovery tests.
Exposure measurement error is potentially more serious with trans fatty acids, though analytical methods for determining trans fatty acid content of foods and tissues, and differentiating ruminant derived from industrially produced trans fatty acids, has evolved considerably since 1980.
The same extraction methods described above for fatty alkane analysis were used for fatty alcohol, except adding 20 μg of 1-pentadecanol as the internal standard.
Cells were prepared and equilibrated similar to the methods described above for fatty acid oxidation, with the exclusion of carnitine from the medium.
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