The method was optimised using a central composite design.
The method was optimised on pure fungal DNA and on plasmid standard dilutions.
The method was optimised by using a central composite experimental design with extraction time, temperature and solvent volume as influential parameters.
An anodic stripping square wave voltammetric method was optimised by factorial design with the conditions of deposition: − 0.8 V for 135 s, and stripping: step height 10 mV, amplitude 50 mV and frequency 13 Hz.
Once the method had been optimised, the influence of the number of extraction cycles was studied.
To our knowledge, this is the first time that USAME method has been optimised for the simultaneous determination of haloanisoles and halophenols in wine.
The method has been optimised for LDV signals measured on bearings of universal electric motors and applied to quality control of washing machines.
In this work, an ultrasound-assisted emulsification microextraction method has been optimised for the determination in wine of haloanisoles (2,4,6-trichloranisole (TCA), 2,3,4,6-tetrachloroanisole (TeCA), 2,4,6-tribromoanisole (TBA) and pentachloranisole (PCA)) responsible for the so-called cork taint.
A dispersive liquid liquid microextraction (DLLME) method has been optimised for simultaneously extracting 2,4,6-trichloranisole (TCA), 2,3,4,6-tetrachloroanisole (TeCA), 2,4,6-tribromoanisole (TBA), pentachloroanisole (PCA), 2,4,6-trichlorophenol (TCP), 2,3,4,6-tetrachlorophenol (TeCP), 2,4,6-tribromophenol (TBP) and pentachlorophenol (PCP) from wine.
This method has been optimised for the characterisation of cloacal bacterial assemblages in kittiwakes [ 13].
