Sentence examples for method development were from inspiring English sources

The output signal was monitored and processed using Empower software version 3. The UPLC columns used during method development were Acquity UPLC BEH-C18 (2.1 mm × 50 mm, 1.7 μm), Acquity CSH phenyl-hexyl (2.1 mm × 100 mm, 1.7 μm), and Acquity UPLC BEH-shield RP18 (3.0 mm × 100 mm, 1.7 μm).

Plasma samples for method development were obtained from healthy volunteers and pooled to ensure anonymity.

Samples, used for method development, were bought in local food shops and proficiency test samples were obtained from the Federal Institute for Risk Assessment (BfR, Berlin, Germany).

In view of the ease of the derivatization and the ensuing chromatographic advantages, further steps in the method development were performed on the thio derivatives of the arsenolipids.

Small-scale fractionations as part of the method development were done with a 200-mL rotor in ascending mode (i.e., lower phase is stationary phase) at 22 °C, a rotation speed of 1,000 rpm, and a flow rate of 10 mL/min.

He said the Secret Service wanted the National Academy "to send a message to the entire forensic science community that this type of method development is not acceptable practice".

The method development is described elsewhere [34], and only a brief description will be given here.

The initial method development was conducted on pure drug using working standards solution protected from light.

The next step in method development was to quantify the degradation rate of the test substances.

Method development was based on a D-optimal experimental design consisting of 16 LPC CHO mixtures.

The method development was carried out on a motorized rotary stage equipped with a Doppler laser instrument.