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Each analysis batch contained 16 unknowns, 2 method blanks, and 2 quality control specimens.
Fortified method blanks and laboratory matrix blanks allow assessment of potential analyte losses from laboratory procedures.
Traceable standards, standard reference material, method blanks, and sample duplicates were processed along with the samples for quality assurance.
Limits of quantification were determined in relation to the method blanks and in relation to the quantification limit of the instrument, which is proportional to the sample size.
The limits of detection (LOD) were defined both in relation to the method blanks and the instrumental detection limit (Sjodin et al. 2004b).
We defined the limit of detection (LOD) in direct relation to the method blanks and the instrumental detection limit (Sjödin et al. 2004).
Similar(50)
Each analytical run consisted of nine unknown specimens, one method blank, and two quality control samples.
Each sample was analyzed five times, and the reported total As value was corrected for any As detected in the method blank and field blank.
Samples were processed in batches of 10, which included a method blank and two quality control samples that were aliquots from pooled bovine sera spiked with PCDDs, PCDFs and co-PCBs.
Breast milk samples were run in batches of 12: nine experimental samples and one duplicate, one method blank, and one quality-control sample from a breast milk pool (QCP).
Samples were processed in batches of 10, which included a method blank and two quality control samples that were aliquots of pooled bovine sera spiked with PCDDs, PCDFs, and C-PCBs.
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