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The peak potential and peak current changed slightly when 3 M methanol was introduced.
Then, in order to improve the contact between P3HT and gold, a PEDOT PSS solution diluted with two volumes of methanol was introduced onto TiO2/CIS/P3HT layer by spin-coating at 2,000 rpm for 30 s[32].
When 3 M methanol was introduced into the O2-saturated alkaline electrolyte at 200 s, no noticeable degradation of current was observed for the NC-6 electrode, as shown in Fig. 8a, whereas a sharp drop in current occurred for the Pt/C electrode.
The post-column reagent (1.2 M KOH in 90% methanol) was introduced using a Waters reagent delivery module and the mixture passed through a 1-ml reaction coil (Waters) kept at 69°C.
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To prevent freezing, 35% methanol is introduced post online digestion.
Water and methanol were introduced to the reactor feed stream using a syringe pump.
A lock mass calibration of sulfadimethoxin at a concentration of 0.05 mg/L in water:methanol (50 50, v/v) was introduced by HPLC pump (LC-10ATVP, Shimadzu, Japan) and split the 60 μL/min to lock spray interface.
After deprotection of the α-amino and carboxylic groups by catalytic hydrogenation in methanol, the Fmoc group was introduced.
A sheath flow consisting of 50% methanol with 0.1% (v/v) formic acid was introduced at a rate of 750 nL/min.
Then, a solution containing phenol, methanol and water in a molar ratio 1 5 1 was introduced into the evaporator.
Fifty milligrams of the tested compound was introduced in 5 ml of methanol.
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