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Methane was added directly to the coal in the reactor, where the microwave energy was applied.
After that, 35 cmethanemethane was added to hydrogen and their mixture flowed into the reactor for 15 min.
The procedure followed for standard resins samples preparation involved the sample dissolution in dichloro methane and subsequent derivatization by diazomethane [44]. 1 mL of dichloro methane was added to a known quantity (1 mg) of sample.
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Therefore, fuel gas (mainly, methane) is added to Claus feed to sustain combustion.
After reaching 1024 °C, the sample was left in H2 for 15 min and then a gradient flux of methane (CH4) was added to the tube for another 15 min (10 sccm for 5 min, 20 sccm for 5 min, 33 sccm for 5 min).
Then 3.37 grams of methane sulfonyl chloride was added dropwise over 90 minutes.
Chlorine was added to methane in the form of methyl chloride gas.
In this study, methane (main component of CNG) was added in two volumetric fractions of 30 and 70% to iso-octane (representative fuel of gasoline).
Two grams of support powders was added into methane solution (40 ml) of PEI, then the mixture was stirred for 2~3 h in a sealed glass vessel and another 6~10 h in fume hood to allow methane evaporation.
The reaction was stirred for 1 h, then further tris-dimethylamino methane (657 mg, 4.53 mmol) was added, and the reaction stirred overnight.
6-Bromo-3,4-dihydro -2H-naphthalen-1-one (204 mg, 0.91 mmol) was dissolved in DMF (2 mL) and tris-dimethylamino methane (657 mg, 4.53 mmol) was added.
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