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Volatile compounds were extracted from this medium using solid-phase micro-extraction and were analysed by gas chromatography/mass spectrometry.
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Nonetheless, efforts to automate organic synthesis using solid-phase methods have begun9.
We synthesized 28 peptides using solid-phase peptide synthesis.
Penicillin residues were derivatised in the crude extract with piperidine and isolated using solid-phase extraction.
The GSLs were then further purified using solid-phase C18 columns (Telos, Kinesis, UK).
Urine was purified using solid phase extraction cartridges.
The extraction recovery using solid phase extraction was 87 98%.
CBZ concentrations were determined using solid phase extraction and LC MS/MS.
The dipeptides were synthesized using solid phase peptide synthesis.
Subsequently, one-step separation using solid phase fractionation was applied.
Thymosin β4 was chemically synthesized on a model 431A peptide synthesizer using solid phase Fmoc chemistry.
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