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Maximum extraction was obtained within the first 200 min (Fig. 5; compared to that of 1200 min duration of the C L tests).

At the optimized condition the maximum chromium extraction was found to be 97.57%.

At the optimized condition the maximum chromium extraction was found to be 89.2% and 96.15% using Trioctyl amine and Aliquat-336, respectively.

The predicted maximum nickel extraction was 31.34% with a pulp density of 8.75%, sucrose concentration of 10.04 g/l, temperature 33.8 °C and duration of 37.5 days.

Maximum likelihood extraction was used to allow generalisation from a sample to a population [ 23] and for correlations with more unique variance and less error variance to be given more weight [ 22].

The determination of a six-factor structure using maximum likelihood extraction was consistent with the previously reported [ 6, 22] and more closely approximate Acute Low Back Pain Screening Questionnaire proposed construct [ 8, 22].

The maximum extraction voltage was designed to be 50 kV.

The maximum extraction time was found to be 60 min.

The maximum extraction yield was found to be 0.8522% w/w at the optimum conditions 300 bar, 308 K, 0.75 mm and 130 min.

In order to achieve the maximum possible concentration in the extract, extraction was performed at high temperatures and columns were connected consecutively in a series.

Different particle sizes in the range of 2.8 mm to ⩽0.5 mm were employed and maximum extraction efficiency was achieved with particles of size ⩽0.5 mm.