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The method validation was completed with spiked matrix samples.
Matrix samples with perforating pores of 40 μm diameter were also studied.
Upstairs, the always popular "Fun With Fossils" activity drew plenty of would-be paleontologists, eager to find cool microfossils in matrix samples collected in Montana.
In particular, a result for the generation of real matrix samples uniformly distributed in the spectral norm ball is presented.
Linearity was studied in the range of 5 200 μg mL−1 for BMV in spiked matrix samples.
The proposed method was successfully applied for the determination of m-nitrophenol, o-nitrophenol and p-nitrophenol in synthetic and real matrix samples such as water.
When determining endogenous compounds in biological samples, the lack of blank or analyte-free matrix samples involves the use of alternative strategies for calibration and quantitation.
This procedure allows the simultaneous determination of nitroaniline isomers in synthetic and real matrix samples good reliability of the determination was proved.
Two matrix samples have been used, characterised by a slightly different relative amount of amine and carboxylic end groups, being the latter predominant in both cases.
Differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) and measurement of heat distortion temperature were also carried out to assess the thermal behavior of the matrix samples.
The limit of detection and limit of quantitation of this method for ZEN and its five primary analogues in various matrix samples ranged from 114.2 to 812.3 ng L−1 and 237.1 to 1653.9 ng L−1, respectively.
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Justyna Jupowicz-Kozak
CEO of Professional Science Editing for Scientists @ prosciediting.com