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When justified, samples were taken and materials analysed by gas chromatography mass spectrometry (GC MS) and/or Fourier transform infrared spectroscopy (FTIR) or cross-sections prepared and studied by analytical microscopic techniques [light microscopy (LM), scanning electron microscopy coupled with energy dispersive X-ray spectroscopy (SEM EDX), and ATR FTIR FPA imaging].
SW conceived of and developed the study (design and all content materials), analysed and interpreted the data and drafted the manuscript.
PK designed and conducted the research, provided materials, analysed data, performed statistical analysis, wrote the paper, and has primary responsibility for final content.
Although further research will be carried out next winter, when the painting will be cleaned and x-rayed, studied by infra-red light, and the pigments and materials analysed in microscopic detail – the £20,000 cost will be funded by the People's Postcode charity lottery – Van de Wetering is convinced it is genuine.
The spectra of these carbonised chars were similar to the spectra obtained from thermally-reduced graphene oxides, especially when compared to a wide range of other carbonaceous materials analysed using this particular methodology.
All data were corrected to the Vienna Pee Dee Belemnite (V-PDB) international scale for δ13C using a 1-point normalisation (i.e. an additive correction) based on the Sigma Aldrich (δ13C: −25.44‰) and IAEA CH-3 (δ13C: −24.724‰) reference materials analysed in each sequence.
Similar(51)
The methodology of materials analyses of the metallurgy of the wire bond interconnects is described.
Ion-milling to produce high quality smooth samples has been used in materials analyses for a considerable time [10] and was investigated here.
And different VCs ask for different materials, analyses and plans.
Samples deriving from wood, biodiesel, solvents and synthetic material analysed by the UBA also all show no resemblance to the homologue patterns in soils.
The same material analysed in reducing SDS gels gave single bands of ~50 kDa.
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Justyna Jupowicz-Kozak
CEO of Professional Science Editing for Scientists @ prosciediting.com