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The mass spectra between m/z 100 and 600, were obtained at a scan speed of 250 m/z.
Comparison of PI mass spectra between urine extracts with control samples in addition to the comparison of PI of MST and its anticipated metabolites (Table 3) resulted in the detection of twenty in vivo phase I and four phase II metabolites (Fig. 2).
For each MALDI plate, the instrument was set to scan mass spectra between 800 and 4000 m/z.
The presence of (E -caryophyllene and gE -caryophyllenein wounded leands was also validated by comparingeranylthe peak retention times and mass spectra between the unknown samplinaloolstandards.
1 While comparing the tandem mass spectra between synthetic standards and experimental peptides, the experiments for unknown peptides and the standard peptides have to be conducted in two separate LC-MS runs.
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The shift in the mass spectrum between the unlabeled compound and the labeled compound indicates the number of atoms in the compounds.
The mass spectrum between 438 and 530 Da was analyzed using 3.0 software flexAnalysis (Bruker Daltonics GmbH, Germany).
The phospholipid fractions were subjected to capillary gas chromatography-mass spectrometry for profiling the phospholipid content in a total run of 45 minutes and full mass spectrum between 100 and 1000 was obtained.
Each mass spectra matching between the spectrum collected and a reference spectrum stored in the database is indicated at the right top corner of each raw spectrum.
The mass spectra analysis alternated between MS and data dependent MS scans using dynamic exclusion.
Mass spectra were processed between 15,000 and 17,000 Da at 1 Da/channel.
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