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The thermogram obtained by heating the green foam in argon showed 62 wt% mass loss occurring in three stages.
Thermogravimetric analyses show that the samples appear to be thermally stable between approximately 650 °C to 1000 °C following an initial mass loss occurring during the first heating cycle.
The first peak began at 225°C, which was most likely due to glycerol degradation (flashpoint of glycerol is around 180°C, with mass loss occurring in nitrogen gas environments at 199°C (Castelló et al. 2009)) within the bioplastic; the peak was right-shifted, most likely due to stabilization in the albumin matrix.
The total organic content was determined from the mass loss occurring up to 500 °C, above which the Fe3O4 oxidizes.
TGA measurements on (1) and (2) (ESI) show the onset of evaporation at ∼380 and 360 K, respectively, with mass loss occurring in a single step for (1), leaving a residue (8.5%) which is unaffected above ∼570 K.
Similar(55)
However, a clear volatilization and mass loss occurred to the organic components under 180 °C for 6 h.
Thus, the mass loss occurred only from the covalently attached PEG on the surface of the MWCNTs.
Above 300°C the weight loss is almost negligible showing that the majority of the mass loss occurs under 300°C which allows for optimization of the calcination temperature.
In the thermal stabilities of FGOs (Figure 3a), the main mass loss occurred from 200°C to 500°C due to the decomposition of the alkylamine moiety [18].
The gasification started by switching nitrogen to carbon dioxide at the desired temperature, and proceeded isothermally until no mass loss occurred.
It was found that during TGA analysis of the carbon matrices (at a temperature range commonly used for soot-in-oil content determination), a gradual mass loss occurred.
Related(14)
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