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Monitoring of cell density requires manual sampling from reactors.
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Figure 10 The correlation of the AUC and peak TAC values obtained by manual sampling and from the flow-through detector.
The correlation of the AUC and peak TAC values obtained by manual sampling and from the flow-through detector is shown in Figure 10.
Both sub-samples from manual sampling and the entire sample from the automatic sampling were coarsely ground using a RAS® (Romer Analytical Sampling, Romerlabs, Tulln, Austria) mill where 96% of the particles passed a 2 mm sieve.
In order to separate the variance resulting from the formation of aggregate samples from the sample reduction data from the manual sampling were reanalysed, using the 'a' analytical sample from each test sample.
Variance from automatic sampling was estimated using data from the eight aggregate samples and variance from the manual sampling, including sample reduction, was estimated using data from the 'a' sub-samples from each aggregate sample.
The probe-derived IF was compared to that obtained from manual sampling at 5-s intervals and IF derived from a left ventricle VOI in a dynamic PET image of the heart.
As expected, the estimates from the standard ANOVA were very sensitive to the inclusion or exclusion of the extreme samples from the manual sampling (M2 and M6) (results not shown).
In general, good agreement was observed between analyses obtained using the portable FIA system and those obtained from manual sampling and laboratory analysis.
These methodologies are used for the estimation of the uncertainty arising from the manual sampling of fuel (automotive diesel) and the subsequent sulfur mass content determination.
The results from the manual sampling clearly showed that not only the nugget effect, but also the spatial distribution may influence sampling uncertainty for OTA.
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