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The obtained solution was stirred for 6 h while maintaining the reaction temperature at 150 °C.
After 4 min of stirring, 2.5 mL AgNO3 solution (0.12 M) and 5 mL polyvinylpyrrolidone (PVP) solution (0.36 M) was added dropwise with maintaining the reaction temperature fixed at 170 °C.
A suspension of LiAlH4 (25 mmol) in anhydrous THF (100 mL) was added dropwise a solution of compounds 2a 8a (20 mmol) in anhydrous THF (50 mL), maintaining the reaction temperature blow 0 °C.
CHX-A″-DTPA conjugation with denatured and intact Cetuximab-Fab was carried out at pH 9.0, maintaining the reaction ratio of CHX-A″-DTPA to Cetuximab-Fab at 10 1.
Briefly, indole, dissolved in ice-cold diethyl ether, was reacted with a solution containing 2 equiv of oxalyl chloride in diethyl ether followed by a 20 wt %/vol solution of dimethylamine in diethyl ether until the pH reached 9 10, while maintaining the reaction mixture at 0 °C with an ice bath.
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The addition rate was carefully controlled to maintain the reaction temperature at 20 °C.
The microwave power was adjusted at 8 W to maintain the reaction mixture at 70 °C.
However, the disadvantage of this system is required to continuously add electron donors (organic molecules) to maintain the reaction since they will be inspired during the photocatalytic reaction.
During the photocatalysis process, the reactor was cooled with a water cooling system to maintain the reaction solution at room temperature.
Immersion of the reaction vessel and associated tubing in a eutectic salt bath and the use of a thermoelectric cooler made it possible to maintain the reaction zone at a constant temperature.
No thermal process would work if too much heat is released or if there is a lack of sufficient thermal energy to drive the process, in order to maintain the reaction temperature.
More suggestions(15)
establishing the reaction
maintaining the test
update the reaction
maintaining the computer
maintaining the ineffectiveness
maintaining the success
maintaining the restaurant
maintaining the clave
maintaining the benefit
maintaining the warehouse
maintaining the prairie
maintaining the battery
maintaining the masking
maintaining the majority
maintaining the regime
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