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The mixture was maintained stirring under room temperature for 10 h to form the white gel.
CP (1.382, 2.765, 3.456 and 4.417 mM) was added to separate vessels containing the 5 %w/w Na-MMT aqueous dispersion (100 cm3) and maintained (stirring) at 50°C for 4 h.
Complete peptization of the precipitate was achieved in the same vessel, maintaining stirring at room temperature for approximately 72 h.
Then, maintaining stirring, 70 ml of 0.1 mol/l aqueous NaOH was added after the mixed system was stirred for 6 h.
Once they reach the desired temperature, maintain the temperature and keep stirring the curds for another 30 minutes.
It is also possible to maintain convective stirring above a cooler bottom layer by a similar slight offset in the temperature settings between the middle and upper sections.
The reaction was allowed to react and maintained under stirring for 12 h.
The reaction was maintained under stirring at room temperature for 5 h, and then placed in an oven at 65 °C for 3 h.
Appropriated amounts of CTAFeII, CTAB, n-butanol, and hexane were mixed until an H value of 0.4 was reached, and then it was maintained under stirring.
In a typical synthesis, solutions of NaOH (9 mol/L) and Ln(NO3 3 (Ln = Ce, La, 0.8 mol/L) were mixed and maintained vigorous stirring for 30 min at room temperature.
Transport from a stagnant bottom-water layer through thermoclines of 15, 10 and 5 °C temperature gradients was studied while maintaining convective stirring above the thermocline with a 250-W aquarium heater.
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