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However, a shift in the calculated d-spacing following dealumination (±3.93 to 3.90 Å for the main reflection in Al-β and deAl-β, respectively) suggests that there is a contraction in unit cell volume following the removal of Al.
After 8, 16, and 24 hours, the crystallinity of the samples returned, but the main reflection in the PXRD showed a change to smaller scattering angles (2 θ≈7.7°).
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(A) Compared with the received signal shown in the sub-figure (b), the MF output in the sub-figure (c) is much closer to the main reflection channel in the sub-figure (a), especially in terms of the magnitude.
As we will show in the next section, the iterative sidelobe removal procedure produces an output y (k) which approximates the main reflection channel (boldsymbol h_{1}^{ k)}).
The X-ray diffractograms of all the films are shown in Figure 7. Neutralized chitosan films show a diffraction pattern of an amorphous structure, similar to the chitosan powder, displaying two main reflections of low intensity in 2θ at 10.5° and 19.8°.
In addition detailed flipcharts recorded the main reflections during the group discussions.
In the last step the restraints were released, resulting in a good fit to the main reflections with R obs = 0.0412.
Thus, the refinement was performed with all main reflections and first-order satellites only.
The evening was also the opening of the main exhibition, "Reflections in a Glass Eye," of works from the center's permanent collection.
The main approaches to reflection in medical education are threefold: a) reflection for learning, b) reflection to develop a therapeutic relationship and c) reflection to develop professional practice.
The μFTIR analysis of painting fragments can be carried out in three main modes: in specular reflection, in Attenuated Total Reflectance (ATR), or in transmission [25].
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Justyna Jupowicz-Kozak
CEO of Professional Science Editing for Scientists @ prosciediting.com