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The cyclic nanoindentation tests were performed in a way with loading to the maximum load and unloading by 90%; reloading to the maximum load and unloading by 9%; holding for 10 s at 10% of the maximum load for thermal drift correction and complete unloading, as illustrated in Fig. 1.
The protocol for one cycle consists of loading to the target peak load, hold for 0.05 s at the peak load, and unloading back to the 0.5 N pre-load.
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