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It was found that the gas and liquid extraction ratio were close to the theoretical value (0.25) and independent of flow patterns, gas and liquid velocities.
The liquid extraction ratio is mainly controlled by the number and diameter of the sampling holes and the gas extraction ratio can be obtained based on the resistance relationship between the main loop and the sample loop.
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It was found that the gas and liquid extraction ratios are very close to the theoretical value (0.167) and independent of inlet flow pattern, gas and liquid velocities.
Extraction ratio.
pressurized liquid extraction.
Based on single factor experiments, investigated liquid ratio, extraction temperature, extraction ph, settlement ph, and extraction time.
The effects of three variables including liquid-solid ratio, extraction time and extraction temperature on the extraction yield of CRPs were taken into consideration.
After optimizing the operating parameters using a Box-Behnken design (BBD), the results showed that the optimal ultrasound-assisted extraction conditions were as follows: extraction temperature, 55 °C; liquid-solid ratio, 25:1; extraction time, 2.2 h; and ultrasound treatment power, 200 W.
Considering the efficiency, the optimum conditions of polysaccharides extraction were liquid:solid ratio of 1 67, immersing time of 10 min, water extraction temperature of 95 °C, and water extraction time of 15 min.
Different parameters of this liquid-liquid extraction (LLE) method had to be optimized, including selection of the extraction solvent, the ratio extraction solvent volume/sample volume or the number of extraction repetitions.
So, concentrations of alcohol, liquid-solid ratio, extraction time, and temperature were selected as the four extraction parameters for the following OAD [ 18].
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