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The resulting CDRs having a remaining reactive chlorine were tested for their capability of derivatizing dl-amino acids followed by liquid chromatographic separation of the resulting diastereomers.
The preconcentration and the subsequent liquid chromatographic separation of tricyclic antidepressants (TCAs) drugs, amitriptyline, imipramine, nortriptyline and desipramine, was carried out with the hyphenated system.
A new class of efficient stationary phase has been investigated for use in the liquid chromatographic separation of low molecular weight analytes and high molecular weight biomolecules, based on the application of immobilised stimuli-responsive polymers (SRPs).
Phospholipase activity was measured with a highly sensitive system that was based on reverse-phase high-performance liquid chromatographic separation of 9-anthracenylmethyl derivatives of fatty acids released by phospholipase A2.
The high-performance liquid chromatographic separation was performed at the flow rate 1.0 min/mL, UV detector wavelength 250 nm and pH of the buffer 3.0 as optimized parameters using design of experiments.
The chromatographic method depends on a high performance liquid chromatographic separation on a reversed-phase C18 column at ambient temperature with mobile phase consisting of 25 mM KH2PO4, pH 3.2 acetonitrile (60 40, v/v).
Similar(27)
Current trends in fast liquid chromatographic separations involve monolith technology, fused core columns, high temperature liquid chromatography and ultra-high performance liquid chromatography (UHPLC).
A simple engineering framework that enables the rapid representation of the performance of liquid chromatographic separations is provided in this paper.
The goal of the present work was to design and implement a simple algorithm for simulation of liquid chromatographic separations that allows for characterization of the effect of injection solvent mismatch and injection solvent volume overload.
Two-dimensional liquid chromatographic separations of blends of silylated linear and hyperbranched polyesters based on 4,4′-hydroxyphenyl-4′- tert-butylmethylsiloxy -phenylvaleric acid were performed using solvent gradient interaction chromatography (SGIC) in the first and size exclusion chromatography (SEC) in the second dimension.
(A) stearidonic acid, methyl ester (standard), (B) S14-2, mester ester (C) linolenic acid, methyl ester (standard), and (D) S14-3, mester ester from reverse-phase, high-performance liquid chromatographic separations that completely superimposed over those of commercial compounds.
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