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The reaction mixture was left to reflux for 24 h.
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Suspensions of SIPPs synthesized using ODA (A), HDA (B), TDA (C), and DDA (D) and allowed to reflux for either 30 or 60 min (left and right vials, respectively).
The mixture was heated to reflux for 1 h.
The mixture was stirred and heated to reflux for 30 min to complete the reaction.
After this time it was heated to reflux for 12 h.
The resulting mixture was heated to reflux for 15 hours.
Final step for esterification was to reflux for 6 hrs.
The reaction mixture was heated to reflux for 24 h.
The mixture was heated to reflux for 45 min.
The mixture was heated to reflux for 2 h.
The reaction was heated to reflux for 2 h and then concentrated to dryness under vacuum.
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