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TPC showed that photogenerated electrons in the BiVO4 layer were extracted within ∼1 ms.
By analyzing the emission spectra, the temporally and spatially resolved electron density and electron temperature at the stagnation layer were extracted, with a time resolution of 10 ns.
The PCB congeners in the hexane layer were extracted with 25 mL DMSO (beforehand saturated with hexane) four times.
The non saponifiable lipids (upper layer) were extracted 5 times with 2 mL of hexane and centrifugation (5,000 × g, 3 min, 4°C).
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After extraction, the resulting top layer was extracted once again with a fresh bottom phase (D3) as before.
The aqueous layer was extracted with Et2O (3 × 30 mL).
Organic layer was separated and aqueous layer was extracted with ethyl acetate (2 × 100 mL).
The organic layer was separated, and the aqueous layer was extracted with Et2O (2 × 15 mL).
After washing with water, the organic layer was extracted and dried over sodium sulfate.
The dichloromethane layer was separated, and the aqueous layer was extracted twice with 4 mL of CH2Cl2.
EtOAc (2 mL) was added to the mixture and aqueous layer was extracted three times with EtOAc (3 mL).
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