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The system was kept at this temperature for 30 minutes.
Then, it was kept at this temperature for 16 h.
The autoclave was heated at 110 °C and kept at this temperature for 8 h.
The reaction was cooled to 10°C and kept at this temperature overnight.
The solution was kept at this temperature until a purple gel was obtained, indicating the formation of P3HT NWs.
CH4/H2 gas mixture was kept at this temperature for 5 min and then was cooled down to 700°C.
The temperature of the system was increased to 875°C and kept at this temperature for 30 min.
Under the Ar blanket, the solution was heated to 240°C and kept at this temperature for 1 h.
Both furnaces were heated to 1123 K and kept at this temperature for dwell time of 1 h.
Subsequently, it was heated to 120° under magnetic stirring and kept at this temperature for 6 h.
The solution was kept at this temperature for 15 min. more after which a test for peroxydisulfate with iodide was negative.
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CEO of Professional Science Editing for Scientists @ prosciediting.com