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It is worth mentioning that the corresponding pyrido[2,3-d]pyrimidines was isolated by crystallization from the crude filtrate.
The blue diamagnetic salts ([Na dme 3]+)2[ 3]2− and ([Na dme 3]+)2[ 4]2− were isolated by crystallization in 52 and 61 % yield, respectively (for detailed synthetic procedures see the Supporting Information).
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Four chiral OsII arene anticancer complexes have been isolated by fractional crystallization.
The N+C complexes were prepared for SEC-MALS as described above for crystallization; 1∶1 complexes were isolated by anion exchange chromatography (HiTrapQ) prior to SEC-MALS analysis.
Thus, urease-positive microorganisms isolated by urinalysis that shows urinary alkalinization and struvite and pyuria crystallization should be considered pathogenic.
Since 7 is soluble, it can be isolated by stirring experiments, while diffusion methods exclusively lead to the crystallization of the completely insoluble polymer 8 at the phase boundary.
This is not surprising because the α2β2 dimer fraction was isolated by SEC, and the dimer is predominant at the concentration of 20 mg/mL used for crystallization.
Each monomer was isolated by column chromatography.
Artemisinin was isolated by pharmacologist Tu Youyou.
Plasma was isolated by centrifugation.
PBMCs were isolated by centrifugation.
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