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The current-time transient shows that the process of reduction is limited by three-dimensional growth of circular cones with progressive nucleation when the potential is stepped from 0.9 to -0.91 V for the anodic film on Pb + 9at.%Bi, but for a thicker film it is also controlled by ion transport through the film.
For A, voltage is stepped from a holding voltage of −110 mV to increasingly more positive voltages (−110 mV–0 mV; ΔV = 10 mV) then returned to the holding voltage of −110 mV.
For D, E and G, voltage is stepped from a holding voltage of −110 mV to increasingly more positive voltages (−110 mV to +70 mV; ΔV = 10 mV) and then returned to the holding voltage of −110 mV.
For D, voltage is stepped from a holding voltage of +80 mV to increasingly more negative voltages (+80 mV to −50 mV; ΔV = −10 mV) then returned to the holding voltage of +80 mV.
For A, B and F, voltage is stepped from a holding voltage of −90 mV to increasingly more positive voltages (−90 mV to +80 mV; ΔV = 10 mV) and then returned to the holding voltage of −90 mV.
For C, voltage is stepped from a holding voltage of −90 mV to increasingly more positive voltages (−90 mV to +80 mV; ΔV = 10 mV) and then returned to −70 mV.
Similar(48)
The 2θ angle was stepped from 5° to 40° at scan rate of 2° min−1.
Presynaptic cells were stepped from Vh = −70 to +20 mV.
The regularization weighting factor α was stepped from 0.001 to 10 in multiples of 10.
For each set of measurements, the NaCl concentration was stepped from lowest (0.1 mM) to highest (500 mM), and the field strength was stepped from lowest (50 V/cm) to highest (250 V/cm).
"Most accidents happen when people are stepping from one wet surface to another," Mr. Mauldin said.
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CEO of Professional Science Editing for Scientists @ prosciediting.com