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Also, the proposed instrument and method present precision equivalent to the Rancimat method (coefficient of variation = 5.0%).
LoDs and LoQs for instrument and method are given in Table 2 Table 2 Instrument and method LoDs and LoQs for determination of Pb, Cd, and Cr in fish feed Parameter Pb Cd Cr Instrument LOD in solution (μg/L) 0.780 0.103 0.221 Instrument LOQ in solution (μg/L) 1.560 0.206 0.442 Method LOD for feed (μg/g) 0.078 0.010 0.022 Method LOQ for feed (μg/g) 0.156 0.021 0.021.
Field validation of the instrument and method was performed in Port Philip and Western Port Bays in Victoria, SE Australia, where 2499 analyses were performed over a 25 h period, over a cruise path of 285 km.
After more than a decade of instrument and method development, broadband coherent anti-Stokes Raman scattering (CARS) micro-spectroscopy is beginning to live up to its potential as a label-free imaging modality that can rapidly generate high resolution images with full vibrational spectra at each image pixel.
Standard bryostatin 1 samples were analyzed using the same instrument and method parameters listed above.
However, we believe that using this instrument and method is our best option to at least gain some insight into the effects of measurement error in these studies.
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The binding of NM23 to MUC1* peptides was also demonstrated using a Biacore surface plasmon resonance (SPR) instrument and methods described in Bamdad [30].
More information about the instrument and methods are available in other publications [ 1, 39].
Analytical validation involves instrument qualification and method validation.
The method was optimised and evaluated for sample preparation, instrument analysis and method performance.
The instruments and methods of flogging have varied.
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