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DHPLC data analysis was by visual inspection of sample and reference chromatograms, with results scored independently by two researchers.
To monitor recording integrity, electrode impedance testing and visual inspection of sample data was performed after the initial hook-up and daily thereafter.
Although it is well-known that decision-making after inspection of sample data can lead to altered Type I and Type II error probabilities and sometimes to spurious rejection of the null hypothesis, researchers are often confused or unaware of the potential shortcomings of such two-stage procedures.
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Higher imaging speeds are desirable for rapid inspection of samples and for the study of a range of dynamic surface processes, such as catalysis and crystal growth.
Manual inspection of samples confirmed this assumption.
Visual inspection of samples collected for this study by the primary author (K.
SEM inspection of samples was performed by a Hitachi S-4800 SEM following Gold coating with a sputter coater (Bal-Tec, Pfäffikon, Switzerland).
A visual inspection of the sample confirmed that sample preparation had not damaged the petal surface, and any samples showing damage or irregularities were discarded.
Inspections of samples disclosed attainable morphologies and also how transitions between morphologies occurred.
All samples have been pre-characterized by SEM. Figure 1 demonstrates the results of SEM inspections of samples A1, a2 (inset), B1, and C1,respectively.
Convergence was checked by visual inspection of the sample trace plots, of posterior density plots and by determining effective sample size using the Coda package in R [ 23].
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