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The inert reaction of LTSD to speech onsets and offsets is quantified by higher values of FEC and OVER in Table 6.
Although some of these protocols provide good yields, they tend to require costly organometallic catalysts, inert reaction conditions, large excesses of reagents [13], long reaction times (>40 h in some instances) and/or complex solvent mixtures.
The resulting dimer with silylated carboxyl group was polycondensed in situ at 300 or 350°C using Marlotherm-S as an inert reaction medium.
The popular routes to synthesize CdSe, whether the west coast method (TBP/TOPO) or the east coast method (TOP/TOPO), generally require rather complicated procedures including delicate control of surfactant ratios and inert reaction conditions due to the toxic and unstable nature of the precursors [25].
This study highlights the largely overlooked influence that seemingly inert reaction mixtures and/or buffer components can potentially have on reaction pathways.
Similar(54)
Results of TPD experiments under inert or reaction atmosphere suggest that the dynamics of SO2 desorption is influenced by the combustion reaction taking place on the catalyst active sites.
10 We only obtained sluggish reactions under an inert atmosphere or in organic solvents (either anhydrous or technical-grade), but the complete conversion of compound 1 a was achieved on water or neat (Table 1, entries 5 and 6).
The results given by both techniques, under inert and reaction conditions, are comparable using the cross-linking pore model.
Acetylated 4,4′-biphenydiol (ABD) and biphenyl-4,4′-dicar☐ylic acid (BDCA) were polycondensed in inert aromatic reaction media at various temperatures and monomer concentrations.
Both measurement techniques, under inert and reaction conditions, have also been carried out with catalyst partially deactivated by coke deposition, with a maximum coke content of 4.5% (w/w) for which the catalyst activity is around 0.1.
With the exception of steel and corium material containing steel, the substances proved relatively inert in reactions with SSiC, such that their use in combination with SSiC can be judged to be favorable.
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