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A-scan values falling below the fifth percentile of the distribution in our normal reference material were transformed through multiplication with an exponential factor.
Methamphetamine hydrochloride and 3,4-methylenedioxymethamphetamine hydrochloride were the in-house reference materials prepared by the Department of Chemistry Malaysia (Petaling Jaya, Malaysia).
Quality control for the analysis included NASS-5 and CASS-4 Certified Reference Materials, in-house reference materials and spike recoveries.
MEL variability in the two in-house reference materials was similar (4% and 6%).
Analyses of in-house reference materials were used for quality assurance.
For quality controls, we used two in-house reference materials (rice and "low-arsenic chicken breast") that were prepared and analyzed in quadruplicate with each batch of samples.
Two infant formula samples, one liquid and one powdered, were used as in-house reference materials; at least one was run in each sample batch.
Only one of the in-house reference materials had appreciable levels of CYA; results from replicate analyses exhibited variability of 18%.
Previous Zn isotope work in our laboratory used an "Imperial Zn" solution prepared from Alfa Aesar Puratronic Zn wire as the in-house reference material [ 9, 37].
Therefore, we argued that appropriate in-house reference material should not only be handled and tested, but also analyzed in a comparable fashion to materials from clinical trials.
Quality control activities consisted of analyses of samples in batches of 10 simultaneously with a blank sample and in-house reference material (spiked porcine serum).
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