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The physical and electrochemical properties of the materials were investigated with variation in final calcination temperature.
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It was found that a transition layer of α-Al2O3 formed in-situ during the final calcination is the best for holding the metal and the catalyst layers together, and that preformed hexaaluminate crystallites are better than those formed during the final calcination.
The clear gel obtained after these steps was then aged at room temperature for 12 24 h and dried at 98 °C for 12 24 h, followed by hydrothermal treatment in a Teflon-lined autoclave at 180 °C for 4 24 h and final calcination in the presence of air up to 600 °C with a temperature ramp of 1 °C min−1.
A four-layer thin films of BiVO4 were deposited by spin coating with intermediate annealing treatment between layers and final calcination at 450 °C in air to shed light on carrier transport in Bi1-x VO4 (s-m).
The process involves in situ growth of magnesium aluminum layered double hydroxides (MgAl-LDHs) in the channels of the γ‐Al2O3 macrospheres by the urea hydrolysis method, followed by calcination, tuning of the basicity through etching of excess aluminum with aqueous alkali and a final calcination step.
At a higher temperature (450°C), equal to the final calcination temperature during catalyst preparation, anionic vacancies were detected at the surface of TiO2 and are in equilibrium with gaseous oxygen.
In this study, top opened nanowires with nanoprotrusions on the surface, which are hierarchical yet single crystalline as a whole, were synthesized by a simple acid treatment at 80 °C for 36 h of hydrothermally synthesized titanate nanowires, followed by a final calcination at 450 °C for 1 h.
After final calcination at 550°C for 1 h, sensitization was achieved by immersing the photoelectrodes in a solution of standard N719 dye (Dyesol Ltd .. Open (non-sealed) DSCs were fabricated by putting a small drop of the novel liquid electrolytes onto the sensitized photoelectrode and simply sandwiching the Pt counter electrode against the first electrode.
In the final step, calcination was performed at 600 °C for 5 h.
In final vote, S.C.
In addition, increase in calcination temperature leads to more crystalline structure [8].
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