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Unless otherwise stated, all reactions were conducted in dried glassware under a positive pressure of dry nitrogen or argon.
Catalysts testing: The catalytic experiments were performed in dried glassware using Schlenk techniques.
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All reactions in anhydrous solvents were carried out in flame-dried glassware under argon.
By using dried glassware, 2- 3- benzyloxy -2-fluorophenyl)- N-(3,4-dimethoxyphenethyl)- N-methylacetamide (1.0 g, 2- 3- benzyloxy -2-fluorophenylacetonitrile (2- 3- benzyloxy -2-fluorophenyl (1.1 g, 7.2- 3- benzyloxy -2-fluorophenylt argon flow.
All moisture sensitive reactions were performed in an inert, dry atmosphere of argon in flame-dried glassware.
All reactions were carried out under an inert atmosphere of nitrogen in oven-dried glassware with magnetic stirring, unless otherwise noted.
Reactions were performed in flame-dried glassware under positive N2 pressure, with magnetic stirring.
All reactions requiring anhydrous conditions were performed in oven-dried glassware under an Ar or N2 atmosphere.
All chemical reactions were carried out under a nitrogen atmosphere in oven-dried glassware using standard techniques.
Air and moisture sensitive reactions were carried out under an inert atmosphere of Ar in oven-dried glassware.
Air- and moisture-sensitive reactions were carried out under an inert atmosphere of argon in oven-dried glassware.
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