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The PPEG-MWNTs/α-CD hydrogel was simply self-assembled with a carbon nanotubes dispersed porphyrin-poly ethylene glycol) solution and an aqueous solution of α-cyclodextrin by homogeneous stirring.
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The solution became clear and homogeneous after stirring for 120 min at 50 to 70°C.
Then, 2.0 M of monoethanolamine (MEA) was added as a sol stabilizer, and acetic acid CH3COOH was dropped to make a homogeneous solution while stirring.
In a typical synthesis, 1.0 g of manganese acetate was put into 30 mL of anhydrous ethanol distilled freshly to form a homogeneous solution under stirring.
Typically, 198 mg MnCl2·4H2O, 582 mg Co(NO3 2·6H2O, 180 mg urea and 37 mg NH4F were dissolved into a beaker containing 40 mL distilled water and 10 mL absolute ethanol to form a homogeneous solution under stirring for 10 min.
FeCl3·6H2O was dissolved into 50 mL ethylene glycol followed by the addition of 3.0 NaAc (protective agent) and 10 mL ethylene diamine (EDA) to form a homogeneous solution with magnetic stirring.
When hydrolysing tetraethoxysilane (TEOS) with tetrapropylammonium hydroxide (TPA-OH), we obtained a homogeneous solution by constant stirring for 6 h at room temperature.
A homogeneous solution was obtained after stirring vigorously for 2 h.
By hydrolyzing TEOS with TPAOH solution, a clear homogeneous solution was obtained under stirring at room temperature for 1 day.
Then, they were mixed at 160 °C for approximately 30 min under stirring to produce homogeneous fiber-modified asphalt mortar.
The temperature was increased to 100 °C to completely dissolve PVA under stirring until a homogeneous solution was obtained.
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