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For the within-bottle homogeneity study, 16 test portions (1 μL) from one same bottle were analysed.
The homogeneity study of the candidate for reference material is essential for the quality of reference material (certified reference material) used in quality assurance activities.
The homogeneity study of candidate for reference materials of contaminated soil collected from a plot situated near the chemical factory "Rokita" in Brzeg Dolny (Silesian Region of Poland) for total metal content of Mg, Fe, Zn, Hg and analytes from a group of polycyclic aromatic hydrocarbons (PAHs), polychlorinated biphenyls (PCBs) was carried out.
Further information regarding the homogeneity test is in the Electronic Supplemental Material (Section 1, Homogeneity study).
The same statistical criteria adopted for the homogeneity study were considered in this study.
The uncertainties derived from material inhomogeneity (ubb) were the estimates in the homogeneity study.
Similar(46)
Aside from the application in homogeneity studies of hair reference materials predominantly in the concentration range of 10 50 pg/mg the method was also designed for daily routine quantification of real-world sample with regard to drinking behavior assessment.
The sample types were subjected to short-term stability (STS), long-term stability (LTS) and homogeneity studies to select the most appropriate concepts for the subsequent steps in the project that resulted in an inter-laboratory comparison.
The most important factor explaining the lack of homogeneity between studies was study quality, with studies of low quality reporting more significant results.
The review was limited to include studies from Western countries to achieve some homogeneity across study populations and health care systems.
We argue that scale-specificity of variables may depend on homogeneity of study areas and should be considered when exploring SOC dynamics.
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