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The 0.3-M DAP solution was added to the 0.3-M calcium hydroxide aqueous suspension in 5 min under high-speed stirring conditions.
Nanoparticles can be prepared by different techniques including solvent emulsification-evaporation, high pressure homogenization, high-speed stirring, ultrasonication, microemulsion using spray-drying, nanoprecipitation and others [29 31].
In brief, P PEGMA -b-P DMAEMA-co-CPLAMA) coP PEGMA -b-P DMAEMA-co-CPLAMAin 1 mL of THF in a 10-mL flask, and then the solution of the P PEGMA -b-P DMAEMA-co-CPLAMAto 6 mL of buffer solutions at desired P PEGMA -b-P DMAEMA-co-CPLAMA
For example, at high-speed stirring (1,800 rpm), discoloration of 3,000 ppm of IC was achieved within 36 h with the aqueous extract of green pea seeds (pH 7.6).
The synthesis of TQ-NLC involves three main major processes that include lipid and aqueous matrices formulation, high-speed stirring by the Ultra-Turrax, and homogenization by the high-pressure homogenizer EmulsiFlex.
At 70°C, 5% of TQ-loaded lipid matrices were dispersed into the aqueous surfactant mixture with high-speed stirring by the Ultra-Turrax (IKA, Staufen, Germany) at 13,000 rpm for 10 minutes to produce a hot preemulsion.
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A stoichiometric amount of TEA was added to the contents of the flask with high speed stirring for 3 h in order to quench HCl produced during the reaction.
The above solution was preserved on high speed stirring for 2 h to get supreme drug released from the particles.
The suspensions were prepared by combining the techniques of high-speed mechanical stirring, ultrasonic agitation and acid oxidation.
After 5 min of high-speed magnetic stirring, a sample was taken from the organic phase to evaluate the residual DBT content and estimate the removal efficiency.
The novel AHP binder was prepared by a copolymerize process using EDA (10 mmol) and HDI (5 mmol) in DMF solvent with high-speed magnetic stirring for 4 h at 60 °C.
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