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Finally, the heating was stopped and the solution allowed to cool down naturally.
After 30 min, heating was stopped and the reaction mixture was left to get cold.
The reaction was allowed to proceed for an additional 15 min (product, platelets), after which heating was stopped.
After 10 min, the heating was stopped and the nanocrystals were precipitated from the reaction mixture by adding methanol followed by centrifugation.
If the heating was stopped when the temperature reached to 1,290°C, nanocables started to nucleate on the substrate (Figure 4c).
In brief, 50 ml of a 0.01% tetrachloroauric acid (HAuCl4) solution was heated under vigorous stirring until boiling; then 600 μl of 1% sodium citrate was added quickly while heating was stopped and stirring was continued.
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"We feel climate change when the local well is dry and the extra heat is stopping the baby from sleeping at night," says Joana. "We have less rain and things grow less".
Subsequently, the heating of the mixture was stopped and the black-brown mixture was cooled down to room temperature (~2 h).
A novel method based on heating the mixture of SnCl2·2H2O and excess S powders in air at 200 240 °C for 0 10 h (t = 0 h, that is, the heating of the reactants was stopped immediately once temperature reached the designed degree), coupled with a subsequent washing treatment, was proposed for the synthesis of SnS2 nanoflakes.
The reaction was stopped heating at 80°C for 20 min, followed by centrifuging at 9880 ×g for 20 min to remove the insoluble portion.
Mr Murakami is feeling the heat: when his taxi was stopped by hordes of journalists in Osaka, he appeared shaken.
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