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In the production of a so-called cemented carbide, such as tungsten carbide, a briquetted mixture of tungsten carbide and cobalt powder is heated at a temperature above the melting point of cobalt.
After being heated at a temperature far above the equilibrium melting point of PEO and cooled down to 318.2±0.1 K, they transformed to the common monoclinic form.
Each sample was heated at a temperature between 250 and 270 °C.
The samples (0.1 g) in hermetically sealed aluminum pans were heated at a temperature range of 20 500 °C at 3 °C/min.
The sample mixture in the round bottom flask was heated at a temperature of 100 °C in a heating mantle for 1 h.
In the oxidation process, trimethylamine N-oxide dehydrate was added to the reactant in a flask, and the mixture was then heated at a temperature of 140 °C for 2 h under a flow of argon.
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The impregnated fabrics are dried, and combination between the reagent and the textile fibres is afterwards effected by heating at a temperature of 100 °-150 ° C. It is the last stage of the process which gives permanence to the proofing.
Then, the samples were dehydrated by heating at a temperature of 600°C for 60 min.
The procedure involves formation of purple colored product by reaction of pregabalin with ninhydrin by heating at a temperature of 70-75°C 70-75°Cminutes.
Then, the composite membrane was taken out and dried in air for 48 h at room temperature followed by heated at a predetermined temperature for certain period to perform the crosslink reaction.
The bottom wall of the channel is heated at a constant temperature and cooled by mixed convection of laminar flow at a relatively low temperature.
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