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Fiber type, extraction temperature, sodium chloride concentration, and headspace volume were the significant variables.
The headspace volume influenced the analytical signals strongly, especially for lower volatile compounds.
SHLPME parameters including nature of extracting solvent, headspace volume and design, extraction time, sample weight and microdrop volume were optimized.
The bubble strip sampling method was examined for various flow rates, bubble sizes (headspace volume in the sampling bulb) and two different H2 concentrations.
The proposed sampler was designed to take a whole headspace volume instead of a portion of it so as to enhance easily the extraction efficiency.
Factors that influenced the IR signals in this method such as the effect of agitation, headspace volume, sample volume, and temperature were examined in this work.
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Headspace volumes for each pot were measured independently.
Headspace volumes for each column were measured independently.
It corresponded to an air renewal rate of one headspace volumes min−1 with an average air flow rate of 0.12 m3 h−1.
According to the results of Pristouri et al. (2010), the exposure of olive oil samples to light, high storage temperatures and large headspace volumes caused the substantial deterioration in product.
The photoreactors consisted of glass tubes with volumes between 14.2 and 14.5 mL with corresponding headspace volumes of 9.7 and 10 mL, respectively.
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