The performance of the microreactor has been characterized through a combination of modeling and experiments including the extraction of kinetics for the oxidation of carbon monoxide.
The film growth has been characterized through the analysis of the temporal evolution of surface roughness, σ, obtained from the AFM data.
The effect of take-up velocity on the structure and properties of as-spun fibers has been characterized through measurements of birefringence, density, wide-angle X-ray diffraction, infrared analysis, DSC melting behavior, tensile properties and high-temperature shrinkage.
The effect of take-up velocity on the structure and properties of as-spun fibers has been characterized through measurements of birefringence, density, wide-angle X-ray scattering, DSC melting behavior, tensile properties and boiling water shrinkage (BWS).
The triclinic crystalline phase with the unit cell parameters a = 7.962 Å, b = 10.006 Å, c = 13.979 Å, α = 96.921°, β = 95.851° and γ = 93.760° has been indexed for TIPO-1 and it has been characterized through powder X-ray diffraction, nitrogen adsorption/desorption, XPS, FT-IR, 31P MAS NMR spectroscopy, UHR-TEM, FE-SEM and TGA/DTA analysis.
The novel oxime derivative (HL) has been characterized through its physical and physicochemical properties such as: melting point (245 248 °C), solubility in water (ca. 2.0 g/l), protonation constant (log Kp, 5.7 in methanol), and an absorption maximum (λmax) in the UV visible spectra, at 365 nm, in methanol solution.
