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Meanwhile, the grains size was refined obviously after rolling deformation.
The grains size of coating was ∼ 10 nm.
After the current annealing, as can be seen in Fig. 3(b) and (c), the roughness of the sample increases alongside with an increase in the grains size.
The mixture of amorphous and nanocrystalline structures with mean grains size less than 10 nm has been observed by HRTEM.
We suppose that a small grains size of the powder is favourable to the pH variations sensitivity.
Two methods to deduce the initial grains size distribution were proposed.
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Grain size frequencies shift towards medium-sized grains.
The maximum grain size, in micro-meters.
The minimum grain size, in micro-meters.
(b) Grain size distribution (average grain size 45 nm) determined from HRTEM images.
Figure 7: Grain size distributions for 14-16 April.
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