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DSC analysis also indicated that the average pore size decreased and the pore size distribution was narrowed with increasing graft time.
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Effects of grafting temperature, grafting time, feed concentration of monomer, and density of –Br on the grafting yields of AAO-g-PNIPAM membranes are systematically investigated.
ATR-FTIR spectra also showed that the grafting degree of styrene was increased with increasing grafting time.
The effects of plasma treatment time, grafting time, grafting temperature and grafting solution concentration on the grafting degree were studied and discussed.
Figure 8 Quantification of sulfonate density as a function of grafting time using dye assay.
Their average hydrodynamic diameter also increases with the prolongation of grafting time.
The sulfonate density as a function of one-step amine grafting time is shown in Figure 8.
The grafting parameters such as absorbed dose, monomer concentration, grafting time and temperature were optimized using response surface method (RS M.
The effects of independent parameters: absorbed dose, monomer concentration, grafting time and reaction temperature on the response, grafting yield (GY) were correlated through two quadratic models.
The optimized grafting parameters; absorbed dose, monomer concentration, grafting time and reaction temperature were varied in four levels to quantify their effect on the grafting yield (GY).
The degree of grafting shows similar trends by ATR-FTIR and ESCA analysis and the optimal grafting time is 4 h.
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