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Gold on carbon catalysts, designed for liquid phase oxidation, have been prepared on 80 500 g scale and evaluated for alcohols and carbohydrates oxidation using glucose and ethane-1,2-diol as model molecules.
The final product was separated on a 1 g scale by silica gel column chromatography using a glass column 20 cm × 2 cm OD packed with 30 g activated silica gel (60-120 mesh).
Figure 3 Reaction scheme for the production of methyl 9, 10-dihydroxyoctadecanoate. Pure methyl 9, 10-dihydroxyoctadecanoate was isolated on a 1 g scale with a yield of 85.10 ± 0.70%.
Some of the aforementioned new compounds were synthesized on a 0.25 2.5 g scale via a 2 to 4 step strategy.
Selected enzymatic hydrolysis results were subsequently replicated at the 500 g scale.
The experiments were run for 7 days, with time course samples taken at 0, 3, 5 and 7 days for 100 g scale experiments, whereas the 500 g scale experiments were only sampled at 0 and 7 days.
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The effectiveness and robustness of the reaction were demonstrated on a 700-g scale.
(A-B, F-G) Scale bars = 0.5 mm; (F-I) Scale bars = 5 μm. Figure 3 Detection of CsPI expressed in transgenic Arabidopsis thaliana plants through quantitative real-time PCR analysis and northern blot analysis.
Navari et al. [ 40] also used the FACT-G scale.
The Cronbach's alpha of the mRRS-G scale was negative.
However, by using the F-G scale to define hairiness and hirsutism, the possible negative effects were reduced.
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