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Various amounts of pentacene (1.3, 3.3, 5.5, 7.7, and 9.9 mg) were dissolved in 3.2 g of NMP solvent.
Assuming that most of the co-solvent resides in the polymer particles, the T g of the solvent-swollen latex particles could be estimated according to the model of Toussaint et al. [ 8].
To estimate solubility, 8 10 mg of compound was dissolved in 1 g of different solvents by vigorous shaking for 1 h and visual control of solubilisation.
The IL-treated cellulose rich substrates were then precipitated by simply adding 6 g of anti-solvent (in our case deionized water) to the pretreated solutions.
The methanolic extract (57 g), after removal of solvent, was dissolved in MeOH-H2O (8 : 2) and partitioned with hexane and ethyl acetate to obtain hexane (16 g), ethyl acetate (7 g), and the remaining hydromethanolic fractions (5 g).
Extraction rate (1: 10 g of flowers powder/mL solvent).
MISO was administered orally (3.0 g m-2) and intravesically (1.0 g in 35 ml of solvent) 4 h and 2 h respectively prior to each fraction of 6 Gy.
Table 2 Yield /YE of solvent free G and other solvent free Lit.
The results of the extraction of 1 g rock with 30 mL of solvent are displayed in Fig. 1.
Briefly, 50 mg of ISO was dissolved in 1.35 g of tetrahydrofuran and chloroform solvent mixture (4:5, w/w).
Fig. 1 Mass fractions (mg/g sediment) and phase associations of mobile elements in the sampled rocks, as determined by sequential extraction with 1 g of rock and 30 mL of solvent.
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