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They identified a unique organic compound in the amber and, using nuclear magnetic resonance spectroscopy, found similarities to fresh resin from a modern tree, Hymenea oblongifolia.
Fresh resin with accelerator is added to cover the cells.
The recycled matrix materials were also combined with fresh resin and cured.
Then, the samples were incubated in 100% fresh resin twice for 8 h, and transferred into fresh resin in an embedding mold and polymerized in a 60°C oven for 3 days.
The next day, fresh resin (100%%) was used for a 2 h infiltration before final embedding and polymerization.
Energy-dispersive X-ray spectroscope (EDX) analysis using SEM was also carried out for elemental analysis of the fresh resin catalyst.
Similar(24)
Modern fresh resins acquired from the Royal Botanic Garden, Sydney, as well as ethnobotanical resins from the Economic Botany Collection at the Royal Botanic Gardens, Kew have formed the reference collection for this research.
Three sets of material were examined: fresh containing virgin fibres and resin, aged which was an out of life but otherwise identical roll and recycled which contained recycled fibre and new resin.
The samples in fresh 100% resin were placed in an oven at 60 °C overnight in order to polymerize the resin.
The orifices were filled with fresh composite resin (simulating the repair).
The samples were embedded in fresh LRW resin in BEEM capsules and polymerized at 60°C for 24 h.
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