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Analysis was conducted by injecting 1 μL of the sample into the programmed temperature vaporizing (PTV) inlet, which followed a temperature program of 60 °C for 1 min, followed by a gradient of 10 °C min−1 up to 370 °C, then held at this temperature for 6 min.
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The general target control parameters for operation of the combustor were as follows: a) temperature 850°C (to mimic the mandatory minimum temperature required for a combustor consuming MSW as a fuel); b) flue gas oxygen content <10% (to indicate operational efficiency); c) duration at least two hours.
Detailed knowledge regarding this mechanism will be useful for efficient all-female cyprinid fish production that follows a temperature-dependent sex determination system.
The results show that, as with the pure heptane droplets, the ignition delay of the NP-laden heptane droplets (n-Al/heptane) followed an Arrhenius temperature dependence.
The oven followed an identical temperature program.
The oven temperature program was held at 40°C for 1 min followed by a temperature ramp of 18°C /min to 250°C, followed by a temperature ramp of 1.5°C /min to a temperature of 260°C, followed by a final temperature ramp of 25°C/min to 300°C which was held for an additional 20 min. The transfer line temperature was maintained at 300°C and the ion source was held at 200°C.
The oven temperature cycle was set as follows: a start temperature of 50 °C was held for 1 min to allow vaporised samples and the solvent (hexane) to condensate at the front of the column.
The temperature program for the analysis was follows: the column was initially held at 100°C for 0.75 min, followed by a temperature gradient of 65°C/min to a temperature of 170°C, where the gradient was decreased to 50°C/min until the temperature reached 300°C.
The reaction involves the interaction between the aluminium acetylacetonate Al acac 3 complex and the silanol surface groups of the PCH, followed by a temperature treatment.
The ln(T) dependence is rather well described by a thermally activated law at elevated temperatures (regime A), with a Δε = 0.25 eV, followed by a temperature regime where the resistivity decreases with lowering the temperature (regime B).
Subsequently, melting curve analysis were performed by heating to 95°C for 0 s, then immediately cooling to 60°C for 30 s, followed by a temperature increase to 95°C (temperature transition rate of 0.5°C/s), while continuously collecting the fluorescence signal data.
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