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Diffraction patterns from the bent polycrystalline Ti6Al4V samples were collected using the new 23-cell "horseshoe" detector and interpreted using Pawley refinement to extract unit cell parameters, thus allowing elastic strain to be determined.
Sorted files were then processed in Neuroexplorer to extract unit timestamps and relevant event markers.
Electrode signals were amplified (×10) through the active bridge circuitry of an Axoprobe-1A amplifier (Molecular Devices Corp ., coupled to alternating current, and further amplified (×100) and bandpass filtered (300 5000 Hz) to extract unit activity (DPA-2FS; Scientifica).
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Due to data protection legislation, we were not permitted to extract unit-specific data.
It is remarkable, however, that the extracted unit cell area of image #12 is in very good agreement with the unit cell area that was extracted by this program from image #10, see Table 5.
The extracted unit cell parameters of this image refer to the oblique Bravais lattice type, while parameters that are compliant with a rectangular (primitive) Bravais lattice type should have been extracted instead.
The areas of the extracted unit cells of these two images in Table 5 are only about one third of the area of the unit cell of the noise-free (and, therefore, less pseudo-symmetric) image in this set, i.e., #7.
Such entries exist only for the CrysTBox and CRISP programs since the PUCE program is not designed to give the user any feedback if the extracted unit cell of a more or less 2D-periodic image might be of the rectangular centered Bravais lattice type.
The only negative thing that could be said about this program is that, typically, error bars on the extracted unit cell angles are at least one order of magnitude larger than one would expect based on the assumption that the CRISP program output are significant numbers.
Bonds must be broken when such a formula unit is extracted from the infinite network, but the broken bonds can all be relinked internally within the extracted unit, retaining all the nearest neighbor topological relationships between the ions and the bonds as shown in Figure 3a for NaCl and Figure 3b for ABX3 perovskite whose structure is shown in Figure 21.
In a subsequent analysis the quality of the extracted units of meaning were rated with scores 1 10 (Fig. 2).
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Justyna Jupowicz-Kozak
CEO of Professional Science Editing for Scientists @ prosciediting.com