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Their curing process can be monitored using experimental tools such as FTIR and DSC; however, these techniques can only provide a qualitative measure of the extent of curing reaction rather than a quantitative determination of cure conversion.
Every 4 5 days mechanical testing was performed and differential scanning calorimetry (DSC) carried out to quantify the extent of curing within samples.
All the samples were able to cure at room temperature, and the extent of curing was dependent on the APTES concentration and curing temperature.
The influence of variables such as extent of curing and length of epoxy strands on elastic response at various temperatures was explored.
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A doctor's value would be measured by the extent of cure achieved.
The overall extent of cure achievable at these temperatures was also higher for the new monomer.
Extent of cure, which is determined by DSC, is used to describe the progress of the polymerization.
The low temperature secondary relaxation peaks were observed to broaden toward higher values with extent of cure.
In some systems cured isothermally at 70°C, the slow cure of the epoxy component allowed the unreacted DGEBA to plasticise the system and enhance the extent of cure of the VER components prior to vitrification of the IPN.
As a consequence of the additional crosslinks introduced by the VER component, premature vitrification occurred during the slower cure of the DGEBA component, thus reducing the extent of cure of the epoxy groups in the IPN.
Dynamic mechanical analysis was performed on the uncured, partially cured, and fully cured samples and a shift in glass transition temperature (Tg) to higher values was observed with extent of cure.
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