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Exposure of the sample is controlled by an electronic shutter.
Carbonates present on the surface after activation were removed after the first exposure of the sample to the nitration flow.
Hence, a prolonged exposure of the sample in the solvent, allowed sufficient time for the desired compounds to migrate into the solvent.
The carbon and oxygen signals observed in the XPS profile are ascribed to the surface contamination during the exposure of the sample to the air before the examination.
The presence of oxygen peak can be attributed to the prolonged exposure of the sample in the air atmosphere [31, 33].
As a consequence, fluorescence acquires a reddish tint at a longer exposure of the sample to UV light (Figure 8, inset).
Similar(35)
Exposure of the samples to air after cleaning is minimized.
Care was taken to minimize exposure of the samples to light during the experiments.
The greatest structural change induced from exposure of the samples to IPA was observed at higher IPA concentrations.
Prolonged exposure of the samples to the electron beam caused damage to the oxide lattice, which transformed into a suboxide.
In order to gain insight into this phenomenon, a series of finite element analyses was performed, simulating the exposure of the samples to the chosen environmental conditions.
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